Hădărugă · Beilstein journal of organic chemistry 2016 · In vitro laboratory experiment · n=?

Thermal and oxidative stability of Atlantic salmon oil (Salmo salar L.) and complexation with β-cyclodextrin.

Cited 39 times in the scientific literature.

Level 5 - mechanism / opinion, no new human data

In vitro bench chemistry study with no human or animal data.

PubMed 26977177 · doi:10.3762/bjoc.12.20 · record verified 2026-08-30

What was done

Atlantic salmon oil was tested for thermal and oxidative stability at temperatures up to 150 °C. The oil was complexed with β-cyclodextrin at host-guest ratios of 1:1 and 3:1 using kneading and ethanol-water co-crystallization methods. Inclusion complex formation was evaluated using thermogravimetry, differential scanning calorimetry, and Karl Fischer titration.

What was found

EPA and DHA degraded significantly even at 50 °C. At 150 °C, relative concentrations decreased from 6.1% to 1.7% for EPA and from 4.1% to 1.5% for DHA. Saturated and monounsaturated fatty acids remained stable or slightly increased in relative proportion (palmitic acid shifted from 10.7% to 12.9%). Differential scanning calorimetry, thermogravimetry, and Karl Fischer titration parameters confirmed inclusion compound formation.

Why it matters

The study quantifies the thermal degradation profile of omega-3 fatty acids in Atlantic salmon oil and shows the feasibility of preparing β-cyclodextrin inclusion complexes for oil encapsulation.

Limits

This is strictly an in vitro laboratory experiment with no biological model. The abstract does not report sample sizes, variance metrics, statistical testing, or direct measurements comparing oxidation rates of encapsulated versus non-encapsulated oil over time.

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