Kynast-Gales · Journal of the American College of Nutrition 1994 · before-after metabolic ward study · n=17

Effect of caffeine on circadian excretion of urinary calcium and magnesium.

Cited 45 times in the scientific literature.

Level 3 - non-randomized controlled study

Non-randomized before-after metabolic study with fixed intervention order

PubMed 7836625 · doi:10.1080/07315724.1994.10718436 · record verified 2026-08-27

What was done

17 healthy male and female volunteers (aged 17–41 years) were studied in a metabolic ward over two consecutive days while consuming a controlled diet (11.3 mmol Ca, 12.7 mmol Mg). Day 1 served as a baseline caffeine-abstinence control. On Day 2, participants consumed two caffeine doses (3 mg/kg lean body mass) at 7:00 AM and 10:00 AM. Researchers measured salivary caffeine concentrations and urinary excretion of calcium, magnesium, sodium, and creatinine across circadian intervals.

What was found

Salivary caffeine peaked at 4.7 µmol/mL at 11:30 AM (half-life 7.3 hours). Urinary calcium and magnesium excretion were significantly elevated during the 6 hours following the second caffeine dose (p = 0.01 and p = 0.04). Excretion was unchanged between 4:00 PM and 1:00 AM, but significantly decreased below baseline between 1:00 AM and 4:00 AM (p = 0.04 for Ca, p = 0.01 for Mg). Creatinine excretion did not change. Nocturnal conservation failed to balance daytime losses, resulting in net 24-hour urinary increases of 0.32 mmol Ca and 0.16 mmol Mg.

Why it matters

This study shows that while the kidneys mount a delayed compensatory response to conserve calcium and magnesium following caffeine-induced excretion, the compensation is incomplete over a 24-hour period.

Limits

Small sample size (n=17). The study used a non-randomized, fixed-order before-after design without a randomized crossover control day. The findings reflect acute effects over 24 hours and do not assess chronic adaptation or bone density outcomes.

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